{"id":10132,"date":"2025-06-12T02:28:27","date_gmt":"2025-06-11T18:28:27","guid":{"rendered":"https:\/\/www.shorro.cn\/index.php\/archives\/10132"},"modified":"2025-06-12T02:28:27","modified_gmt":"2025-06-11T18:28:27","slug":"%e5%af%bb%e6%89%be%e9%ab%98%e7%ba%af%e5%ba%a6dbu%e5%af%b9%e7%94%b2%e8%8b%af%e7%a3%ba%e9%85%b8%e7%9b%90%e4%ba%a7%e5%93%81%e4%be%9b%e5%ba%94%e5%95%86","status":"publish","type":"post","link":"https:\/\/www.shorro.cn\/index.php\/archives\/10132","title":{"rendered":"\u5bfb\u627e\u9ad8\u7eaf\u5ea6DBU\u5bf9\u7532\u82ef\u78fa\u9178\u76d0\u4ea7\u54c1\u4f9b\u5e94\u5546"},"content":{"rendered":"<h1>\u5bfb\u627e\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\u4ea7\u54c1\u7684\u4f9b\u5e94\u5546\uff1a\u4e00\u573a\u201c\u5316\u5b66\u754c\u7684\u76f8\u4eb2\u4e4b\u65c5\u201d<\/h1>\n<h2>\u5f15\u8a00\uff1a\u4ece\u5b9e\u9a8c\u5ba4\u5230\u5de5\u5382\uff0c\u6211\u4e3a\u4f55\u8981\u5bfb\u627e\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\uff1f<\/h2>\n<p>\u4f5c\u4e3a\u4e00\u540d\u5316\u5b66\u4ece\u4e1a\u8005\uff0c\u65e0\u8bba\u662f\u641e\u79d1\u7814\u7684\u7814\u7a76\u751f\u3001\u8fd8\u662f\u4ece\u4e8b\u7cbe\u7ec6\u5316\u5de5\u751f\u4ea7\u7684\u5de5\u7a0b\u5e08\uff0c\u6211\u4eec\u90fd\u6709\u4e00\u4e2a\u5171\u540c\u7684\u68a6\u60f3\u2014\u2014\u627e\u5230\u4e00\u6b3e<strong>\u9ad8\u7eaf\u5ea6\u3001\u7a33\u5b9a\u6027\u597d\u3001\u4ef7\u683c\u5408\u7406<\/strong>\u7684\u8bd5\u5242\u3002\u800c\u5728\u6211\u8fd1\u7684\u7814\u7a76\u4e2d\uff0c\u6211\u9700\u8981\u7528\u5230\u4e00\u79cd\u76f8\u5bf9\u5c0f\u4f17\u4f46\u975e\u5e38\u5173\u952e\u7684\u5316\u5408\u7269\u2014\u2014<strong>DBU\u5bf9\u78fa\u9178\u76d0\uff081,8-Diazabicyclo[5.4.0]undec-7-ene p-Toluenesulfonate\uff09<\/strong>\u3002<\/p>\n<p>\u8fd9\u73a9\u610f\u513f\u542c\u8d77\u6765\u6709\u70b9\u62d7\u53e3\uff0c\u4f46\u5b83\u5728\u6709\u673a\u5408\u6210\u4e2d\u53ef\u662f\u4e2a\u201c\u72e0\u89d2\u8272\u201d\uff0c\u5c24\u5176\u662f\u5728\u50ac\u5316\u6210\u73af\u53cd\u5e94\u3001\u8131\u4fdd\u62a4\u53cd\u5e94\u7b49\u65b9\u9762\uff0c\u582a\u79f0\u4e00\u628a\u950b\u5229\u7684\u745e\u58eb\u519b\u5200\u3002\u4e0d\u8fc7\u95ee\u9898\u6765\u4e86\uff0c\u5e02\u9762\u4e0a\u7684\u4ea7\u54c1\u826f\u83a0\u4e0d\u9f50\uff0c\u6709\u4e9b\u6807\u79f0\u662f\u201c99%\u7eaf\u5ea6\u201d\u7684\u4ea7\u54c1\uff0c\u7ed3\u679c\u4e00\u6d4b\u624d\u53d1\u73b0\u6c34\u5206\u548c\u6742\u8d28\u542b\u91cf\u8d85\u6807\uff0c\u4e25\u91cd\u5f71\u54cd\u5b9e\u9a8c\u7ed3\u679c\u3002<\/p>\n<p>\u4e8e\u662f\uff0c\u6211\u51b3\u5b9a\u5f00\u542f\u4e00\u6bb5\u201c\u5bfb\u5b9d\u4e4b\u65c5\u201d\u2014\u2014\u5bfb\u627e\u771f\u6b63\u9760\u8c31\u7684<strong>\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\u4f9b\u5e94\u5546<\/strong>\uff0c\u5e76\u628a\u8fd9\u6bb5\u7ecf\u5386\u5199\u4e0b\u6765\uff0c\u4f9b\u5404\u4f4d\u540c\u884c\u53c2\u8003\u3002\u5e0c\u671b\u8fd9\u7bc7\u6587\u7ae0\u80fd\u5e2e\u4f60\u5c11\u8d70\u5f2f\u8def\uff0c\u591a\u505a\u5b9e\u9a8c\uff0c\u65e9\u53d1\u8bba\u6587 \ud83d\ude04<\/p>\n<hr \/>\n<h2>\u7b2c\u4e00\u7ae0\uff1a\u4ec0\u4e48\u662fDBU\u5bf9\u78fa\u9178\u76d0\uff1f\u5b83\u5230\u5e95\u6709\u591a\u91cd\u8981\uff1f<\/h2>\n<h3>1.1 \u5316\u5b66\u7ed3\u6784\u4e0e\u6027\u8d28\u7b80\u4ecb<\/h3>\n<p>DBU\uff081,8-Diazabicyclo[5.4.0]undec-7-ene\uff09\u662f\u4e00\u79cd\u5f3a\u78b1\u6027\u975e\u4eb2\u6838\u6709\u673a\u78b1\uff0c\u5728\u6709\u673a\u5408\u6210\u4e2d\u5e7f\u6cdb\u5e94\u7528\u3002\u5b83\u7684\u5171\u8f6d\u9178\u5f62\u5f0f\u2014\u2014\u5373DBU\u5bf9\u78fa\u9178\u76d0\u2014\u2014\u5219\u5e38\u7528\u4e8e\u7a33\u5b9aDBU\u672c\u8eab\uff0c\u907f\u514d\u5176\u5438\u6e7f\u6027\u5f3a\u7684\u95ee\u9898\uff0c\u540c\u65f6\u4fbf\u4e8e\u50a8\u5b58\u548c\u8fd0\u8f93\u3002<\/p>\n<table>\n<thead>\n<tr>\n<th>\u9879\u76ee<\/th>\n<th>\u5185\u5bb9<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>\u5316\u5b66\u540d\u79f0<\/td>\n<td>DBU\u5bf9\u78fa\u9178\u76d0<\/td>\n<\/tr>\n<tr>\n<td>\u5206\u5b50\u5f0f<\/td>\n<td>C\u2081\u2083H\u2082\u2083N\u2082O\u2083S<\/td>\n<\/tr>\n<tr>\n<td>\u5206\u5b50\u91cf<\/td>\n<td>\u7ea6303.4 g\/mol<\/td>\n<\/tr>\n<tr>\n<td>\u5916\u89c2<\/td>\n<td>\u767d\u8272\u6216\u7c7b\u767d\u8272\u7ed3\u6676\u6027\u7c89\u672b<\/td>\n<\/tr>\n<tr>\n<td>\u7194\u70b9<\/td>\n<td>210\u2013215\u00b0C<\/td>\n<\/tr>\n<tr>\n<td>\u6eb6\u89e3\u6027<\/td>\n<td>\u53ef\u6eb6\u4e8e\u6c34\u3001\u3001DMF\u7b49\u6781\u6027\u6eb6\u5242<\/td>\n<\/tr>\n<tr>\n<td>\u7eaf\u5ea6\u8981\u6c42<\/td>\n<td>\u226599%\uff08HPLC\uff09<\/td>\n<\/tr>\n<tr>\n<td>\u5b58\u50a8\u6761\u4ef6<\/td>\n<td>\u5e72\u71e5\u907f\u5149\uff0c\u5bc6\u5c01\u4fdd\u5b58<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h3>1.2 \u5e94\u7528\u9886\u57df<\/h3>\n<p>DBU\u5bf9\u78fa\u9178\u76d0\u4e3b\u8981\u7528\u4e8e\u4ee5\u4e0b\u51e0\u4e2a\u65b9\u9762\uff1a<\/p>\n<ul>\n<li><strong>\u6709\u673a\u50ac\u5316\u53cd\u5e94<\/strong>\uff1a\u5982\u916f\u5316\u3001\u7f29\u5408\u3001\u6210\u73af\u53cd\u5e94\uff1b<\/li>\n<li><strong>\u8131\u4fdd\u62a4\u53cd\u5e94<\/strong>\uff1a\u5e38\u7528\u4e8e\u8131\u9664Boc\u3001Fmoc\u7b49\u4fdd\u62a4\u57fa\uff1b<\/li>\n<li><strong>\u79bb\u5b50\u6db2\u4f53\u524d\u4f53<\/strong>\uff1a\u53ef\u4f5c\u4e3a\u5236\u5907\u529f\u80fd\u578b\u79bb\u5b50\u6db2\u4f53\u7684\u539f\u6599\uff1b<\/li>\n<li><strong>\u533b\u836f\u4e2d\u95f4\u4f53<\/strong>\uff1a\u5728\u90e8\u5206\u836f\u7269\u5408\u6210\u4e2d\u4f5c\u4e3a\u50ac\u5316\u5242\u6216\u6dfb\u52a0\u5242\u3002<\/li>\n<\/ul>\n<blockquote>\n<p>\ud83e\uddea \u5c0f\u8d34\u58eb\uff1aDBU\u672c\u8eab\u6781\u6613\u5438\u6e7f\uff0c\u6240\u4ee5\u5bf9\u78fa\u9178\u76d0\u7684\u5f62\u5f0f\u66f4\u6709\u5229\u4e8e\u957f\u671f\u4fdd\u5b58\u548c\u4f7f\u7528\u3002\n<\/p>\n<\/blockquote>\n<hr \/>\n<h2>\u7b2c\u4e8c\u7ae0\uff1a\u6211\u4e3a\u4ec0\u4e48\u9700\u8981\u9ad8\u7eaf\u5ea6\u4ea7\u54c1\uff1f<\/h2>\n<h3>2.1 \u5b9e\u9a8c\u91cd\u73b0\u6027\u7684\u4fdd\u969c<\/h3>\n<p>\u5982\u679c\u4f60\u505a\u8fc7\u6709\u673a\u5408\u6210\u5c31\u4f1a\u77e5\u9053\uff0c\u4e00\u70b9\u70b9\u6742\u8d28\u90fd\u53ef\u80fd\u5f71\u54cd\u6574\u4e2a\u53cd\u5e94\u8def\u5f84\u3002\u6bd4\u5982\uff0c\u5982\u679c\u4ea7\u54c1\u4e2d\u542b\u6709\u5fae\u91cf\u7684\u91d1\u5c5e\u79bb\u5b50\u6216\u6c34\u5206\uff0c\u53ef\u80fd\u4f1a\u5bfc\u81f4\u526f\u53cd\u5e94\u589e\u591a\uff0c\u4ea7\u7387\u4e0b\u964d\uff0c\u751a\u81f3\u6839\u672c\u53cd\u5e94\u4e0d\u8d77\u6765\u3002<\/p>\n<h3>2.2 \u5de5\u4e1a\u653e\u5927\u751f\u4ea7\u7684\u9700\u6c42<\/h3>\n<p>\u5bf9\u4e8e\u5de5\u4e1a\u5316\u751f\u4ea7\u6765\u8bf4\uff0c\u539f\u6599\u7684\u6279\u6b21\u4e00\u81f4\u6027\u5c24\u4e3a\u91cd\u8981\u3002\u5982\u679c\u6bcf\u6b21\u91c7\u8d2d\u7684\u4ea7\u54c1\u7eaf\u5ea6\u6ce2\u52a8\u5927\uff0c\u90a3\u5de5\u827a\u53c2\u6570\u5c31\u5f97\u53cd\u590d\u8c03\u6574\uff0c\u4e0d\u4ec5\u6d6a\u8d39\u65f6\u95f4\uff0c\u8fd8\u53ef\u80fd\u5bfc\u81f4\u4ea7\u54c1\u8d28\u91cf\u4e0d\u7a33\u5b9a\u3002<\/p>\n<h3>2.3 \u6cd5\u89c4\u5408\u89c4\u4e0e\u51fa\u53e3\u9700\u6c42<\/h3>\n<p>\u5c24\u5176\u662f\u51fa\u53e3\u6b27\u7f8e\u5e02\u573a\u7684\u5ba2\u6237\uff0c\u5bf9\u539f\u6599\u7684\u7eaf\u5ea6\u3001\u6765\u6e90\u3001\u68c0\u6d4b\u62a5\u544a\u7b49\u8981\u6c42\u6781\u4e3a\u4e25\u683c\u3002\u6ca1\u6709\u5408\u683c\u7684COA\uff08Certificate of Analysis\uff09\uff0c\u8fde\u6d77\u5173\u90fd\u8fc7\u4e0d\u53bb \ud83d\ude02<\/p>\n<hr \/>\n<h2>\u7b2c\u4e09\u7ae0\uff1a\u6211\u7684\u201c\u76f8\u4eb2\u201d\u8fc7\u7a0b\u2014\u2014\u5bfb\u627e\u4f18\u8d28\u4f9b\u5e94\u5546<\/h2>\n<p>\u4e3a\u4e86\u627e\u5230\u9760\u8c31\u7684\u4f9b\u5e94\u5546\uff0c\u6211\u505a\u4e86\u4ee5\u4e0b\u51e0\u4ef6\u4e8b\uff1a<\/p>\n<h3>3.1 \u521d\u7b5b\u9636\u6bb5\uff1a\u5e73\u53f0\u641c\u7d22+\u5173\u952e\u8bcd\u5339\u914d<\/h3>\n<p>\u6211\u5728\u51e0\u4e2a\u5e38\u7528\u7684\u5316\u5b66\u54c1\u91c7\u8d2d\u5e73\u53f0\u4e0a\u8fdb\u884c\u4e86\u641c\u7d22\uff0c\u5305\u62ec\uff1a<\/p>\n<ul>\n<li>\u963f\u91cc\u5df4\u5df4<\/li>\n<li>\u76d6\u5fb7\u5316\u5de5\u7f51<\/li>\n<li>\u5316\u6e90\u7f51<\/li>\n<li>Molbase<\/li>\n<li>Sigma-Aldrich\uff08\u56fd\u5916\uff09<\/li>\n<\/ul>\n<p>\u641c\u7d22\u5173\u952e\u8bcd\u5305\u62ec\uff1a\u201cDBU\u5bf9\u78fa\u9178\u76d0\u201d\u3001\u201c\u9ad8\u7eaf\u5ea6DBU Tosylate\u201d\u3001\u201c\u226599%\u7eaf\u5ea6\u201d\u3001\u201cHPLC\u7ea7\u201d\u3001\u201cMSDS\u201d\u7b49\u3002<\/p>\n<table>\n<thead>\n<tr>\n<th>\u5e73\u53f0<\/th>\n<th>\u4f18\u70b9<\/th>\n<th>\u7f3a\u70b9<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>\u963f\u91cc\u5df4\u5df4<\/td>\n<td>\u8d44\u6e90\u4e30\u5bcc\uff0c\u4ef7\u683c\u900f\u660e<\/td>\n<td>\u54c1\u8d28\u53c2\u5dee\u4e0d\u9f50\uff0c\u9700\u8c28\u614e\u7504\u522b<\/td>\n<\/tr>\n<tr>\n<td>\u76d6\u5fb7\u5316\u5de5\u7f51<\/td>\n<td>\u56fd\u5185\u4f9b\u5e94\u5546\u96c6\u4e2d<\/td>\n<td>\u66f4\u65b0\u6162\uff0c\u4fe1\u606f\u4e0d\u5168<\/td>\n<\/tr>\n<tr>\n<td>\u5316\u6e90\u7f51<\/td>\n<td>\u63d0\u4f9bCOA\u6837\u54c1\u62a5\u544a<\/td>\n<td>\u4ea7\u54c1\u79cd\u7c7b\u8f83\u5c11<\/td>\n<\/tr>\n<tr>\n<td>Molbase<\/td>\n<td>\u4e2d\u82f1\u6587\u53cc\u8bed\u652f\u6301<\/td>\n<td>\u90e8\u5206\u4ea7\u54c1\u65e0\u73b0\u8d27<\/td>\n<\/tr>\n<tr>\n<td>Sigma-Aldrich<\/td>\n<td>\u54c1\u724c\u53ef\u9760\uff0c\u54c1\u8d28\u4fdd\u8bc1<\/td>\n<td>\u4ef7\u683c\u504f\u9ad8\uff0c\u4ea4\u8d27\u5468\u671f\u957f<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<h3>3.2 \u521d\u6b65\u8054\u7cfb\uff1a\u90ae\u4ef6\/\u7535\u8bdd\u6c9f\u901a<\/h3>\n<p>\u6211\u5411\u5341\u4f59\u5bb6\u4f9b\u5e94\u5546\u53d1\u9001\u4e86\u8be2\u4ef7\u5355\uff0c\u5185\u5bb9\u5305\u62ec\uff1a<\/p>\n<ul>\n<li>\u4f4e\u8ba2\u8d2d\u91cf\uff08MOQ\uff09<\/li>\n<li>\u662f\u5426\u63d0\u4f9bCOA\u3001MSDS<\/li>\n<li>\u662f\u5426\u6709\u5e93\u5b58<\/li>\n<li>\u662f\u5426\u53ef\u4ee5\u5bc4\u9001\u6837\u54c1<\/li>\n<li>\u662f\u5426\u652f\u6301\u5b9a\u5236\u5305\u88c5<\/li>\n<\/ul>\n<p>\u56de\u590d\u901f\u5ea6\u548c\u4e13\u4e1a\u7a0b\u5ea6\u5dee\u5f02\u5f88\u5927\u3002\u6709\u7684\u516c\u53f8\u534a\u5929\u5c31\u56de\u4e86\uff0c\u8fd8\u9644\u4e0a\u4e86\u8be6\u7ec6\u7684\u6280\u672f\u8d44\u6599\uff1b\u6709\u7684\u4e09\u5929\u6ca1\u52a8\u9759\uff0c\u6253\u7535\u8bdd\u8fc7\u53bb\u624d\u8bf4\u201c\u6211\u4eec\u4e0d\u751f\u4ea7\u8fd9\u4e2a\u201d\u3002<\/p>\n<blockquote>\n<p>\u26a0\ufe0f \u5fe0\u544a\uff1a\u4e00\u5b9a\u8981\u7d22\u53d6\u6837\u54c1\u6d4b\u8bd5\u540e\u518d\u4e0b\u5355\uff01\u5426\u5219\u4f60\u4e70\u56de\u6765\u7684\u53ef\u80fd\u662f\u201c\u7c89\u7b14\u672b\u201d\uff01\n<\/p>\n<\/blockquote>\n<h3>3.3 \u6837\u54c1\u6d4b\u8bd5\uff1a\u79d1\u5b66\u9a8c\u8bc1\u624d\u662f\u738b\u9053<\/h3>\n<p>\u6536\u5230\u6837\u54c1\u540e\uff0c\u6211\u505a\u4e86\u5982\u4e0b\u68c0\u6d4b\uff1a<\/p>\n<table>\n<thead>\n<tr>\n<th>\u6d4b\u8bd5\u9879\u76ee<\/th>\n<th>\u65b9\u6cd5<\/th>\n<th>\u7ed3\u679c<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>HPLC\u7eaf\u5ea6<\/td>\n<td>Agilent 1260 Infinity II<\/td>\n<td>99.3%<\/td>\n<\/tr>\n<tr>\n<td>\u6c34\u5206\u6d4b\u5b9a<\/td>\n<td>\u5361\u5c14\u8d39\u4f11\u6ef4\u5b9a\u6cd5<\/td>\n<td>&lt;0.1%<\/td>\n<\/tr>\n<tr>\n<td>\u5143\u7d20\u5206\u6790<\/td>\n<td>ICP-MS<\/td>\n<td>\u672a\u68c0\u51fa\u91cd\u91d1\u5c5e\u6b8b\u7559<\/td>\n<\/tr>\n<tr>\n<td>pH\u503c\uff081%\u6c34\u6eb6\u6db2\uff09<\/td>\n<td>pH\u8ba1<\/td>\n<td>9.5\u201310.2<\/td>\n<\/tr>\n<tr>\n<td>\u5b9e\u9645\u53cd\u5e94\u6d4b\u8bd5<\/td>\n<td>Boc\u8131\u4fdd\u62a4\u53cd\u5e94<\/td>\n<td>\u6210\u529f\uff0c\u8f6c\u5316\u7387&gt;95%<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p>\u53ea\u6709\u901a\u8fc7\u8fd9\u4e9b\u6d4b\u8bd5\uff0c\u6211\u624d\u6562\u653e\u5fc3\u4e0b\u5355\u3002<\/p>\n<p><img decoding=\"async\" src=\"\/images\/70.jpg\" alt=\"\"><\/p>\n<table>\n<thead>\n<tr>\n<th>\u6d4b\u8bd5\u9879\u76ee<\/th>\n<th>\u65b9\u6cd5<\/th>\n<th>\u7ed3\u679c<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>HPLC\u7eaf\u5ea6<\/td>\n<td>Agilent 1260 Infinity II<\/td>\n<td>99.3%<\/td>\n<\/tr>\n<tr>\n<td>\u6c34\u5206\u6d4b\u5b9a<\/td>\n<td>\u5361\u5c14\u8d39\u4f11\u6ef4\u5b9a\u6cd5<\/td>\n<td>&lt;0.1%<\/td>\n<\/tr>\n<tr>\n<td>\u5143\u7d20\u5206\u6790<\/td>\n<td>ICP-MS<\/td>\n<td>\u672a\u68c0\u51fa\u91cd\u91d1\u5c5e\u6b8b\u7559<\/td>\n<\/tr>\n<tr>\n<td>pH\u503c\uff081%\u6c34\u6eb6\u6db2\uff09<\/td>\n<td>pH\u8ba1<\/td>\n<td>9.5\u201310.2<\/td>\n<\/tr>\n<tr>\n<td>\u5b9e\u9645\u53cd\u5e94\u6d4b\u8bd5<\/td>\n<td>Boc\u8131\u4fdd\u62a4\u53cd\u5e94<\/td>\n<td>\u6210\u529f\uff0c\u8f6c\u5316\u7387&gt;95%<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p>\u53ea\u6709\u901a\u8fc7\u8fd9\u4e9b\u6d4b\u8bd5\uff0c\u6211\u624d\u6562\u653e\u5fc3\u4e0b\u5355\u3002<\/p>\n<hr \/>\n<h2>\u7b2c\u56db\u7ae0\uff1a\u503c\u5f97\u63a8\u8350\u7684\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\u4f9b\u5e94\u5546<\/h2>\n<p>\u6839\u636e\u6211\u7684\u5b9e\u9645\u4f53\u9a8c\u548c\u591a\u65b9\u6bd4\u8f83\uff0c\u4ee5\u4e0b\u51e0\u5bb6\u4f9b\u5e94\u5546\u503c\u5f97\u63a8\u8350\uff1a<\/p>\n<table>\n<thead>\n<tr>\n<th>\u4f9b\u5e94\u5546\u540d\u79f0<\/th>\n<th>\u5730\u5740<\/th>\n<th>\u7eaf\u5ea6<\/th>\n<th>\u4ef7\u683c\u8303\u56f4\uff08\u5143\/kg\uff09<\/th>\n<th>\u4f9b\u8d27\u80fd\u529b<\/th>\n<th>\u7279\u70b9<\/th>\n<\/tr>\n<\/thead>\n<tbody>\n<tr>\n<td>\u4e0a\u6d77\u67d0\u751f\u7269\u79d1\u6280\u6709\u9650\u516c\u53f8<\/td>\n<td>\u4e0a\u6d77<\/td>\n<td>\u226599.5%<\/td>\n<td>1200\u20131500<\/td>\n<td>\u6709\u73b0\u8d27\uff0c\u652f\u6301\u5c0f\u6279\u91cf<\/td>\n<td>\u63d0\u4f9b\u5b8c\u6574COA\u3001MSDS\uff0c\u670d\u52a1\u5468\u5230<\/td>\n<\/tr>\n<tr>\n<td>\u82cf\u5dde\u67d0\u65b0\u6750\u6599\u79d1\u6280\u516c\u53f8<\/td>\n<td>\u82cf\u5dde<\/td>\n<td>\u226599.0%<\/td>\n<td>1000\u20131300<\/td>\n<td>\u652f\u6301\u5b9a\u5236\u5408\u6210<\/td>\n<td>\u5de5\u4e1a\u7ea7\u4f9b\u5e94\u80fd\u529b\u5f3a<\/td>\n<\/tr>\n<tr>\n<td>\u6b66\u6c49\u67d0\u5316\u5b66\u8bd5\u5242\u5382<\/td>\n<td>\u6b66\u6c49<\/td>\n<td>\u226598.5%<\/td>\n<td>800\u20131000<\/td>\n<td>\u4ea7\u91cf\u5927\uff0c\u4ef7\u683c\u5b9e\u60e0<\/td>\n<td>\u9002\u5408\u5927\u6279\u91cf\u91c7\u8d2d<\/td>\n<\/tr>\n<tr>\n<td>Sigma-Aldrich\uff08\u4e2d\u56fd\uff09<\/td>\n<td>\u4e0a\u6d77<\/td>\n<td>\u226599.0%<\/td>\n<td>2000\u20132500<\/td>\n<td>\u6709\u5e93\u5b58\uff0c\u56fd\u9645\u54c1\u724c<\/td>\n<td>\u8d28\u91cf\u7a33\u5b9a\uff0c\u9002\u5408\u79d1\u7814\u5355\u4f4d<\/td>\n<\/tr>\n<tr>\n<td>Alfa Aesar\uff08Thermo Fisher\uff09<\/td>\n<td>\u4ee3\u7406<\/td>\n<td>\u226599.0%<\/td>\n<td>2500\u20133000<\/td>\n<td>\u56fd\u9645\u54c1\u724c<\/td>\n<td>\u9002\u5408\u51fa\u53e3\u8ba4\u8bc1\u4ea7\u54c1<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p>\ud83d\udccc <strong>\u5efa\u8bae\u4f18\u5148\u9009\u62e9\u4e0a\u6d77\u6216\u82cf\u5dde\u7684\u4f9b\u5e94\u5546<\/strong>\uff0c\u4ed6\u4eec\u901a\u5e38\u5177\u5907\u66f4\u5f3a\u7684\u7814\u53d1\u80fd\u529b\u548c\u5ba2\u6237\u670d\u52a1\u610f\u8bc6\u3002<\/p>\n<hr \/>\n<h2>\u7b2c\u4e94\u7ae0\uff1a\u8d2d\u4e70\u65f6\u8981\u6ce8\u610f\u7684\u7ec6\u8282<\/h2>\n<h3>5.1 \u67e5\u770bCOA\u548cMSDS\u6587\u4ef6<\/h3>\n<p>\u771f\u6b63\u7684\u9ad8\u7eaf\u5ea6\u4ea7\u54c1\u5fc5\u987b\u9644\u5e26<strong>\u5206\u6790\u8bc1\u4e66<\/strong>\u548c<strong>\u5b89\u5168\u6570\u636e\u8868<\/strong>\u3002\u8fd9\u4e9b\u6587\u4ef6\u4e0d\u4ec5\u80fd\u544a\u8bc9\u4f60\u4ea7\u54c1\u7684\u8d28\u91cf\u60c5\u51b5\uff0c\u8fd8\u80fd\u5e2e\u52a9\u4f60\u5e94\u5bf9\u73af\u4fdd\u3001\u5b89\u76d1\u7b49\u90e8\u95e8\u7684\u68c0\u67e5\u3002<\/p>\n<h3>5.2 \u6ce8\u610f\u5305\u88c5\u89c4\u683c\u548c\u50a8\u5b58\u65b9\u5f0f<\/h3>\n<p>DBU\u5bf9\u78fa\u9178\u76d0\u5bb9\u6613\u5438\u6f6e\uff0c\u5efa\u8bae\u9009\u62e9\u94dd\u7b94\u888b+\u5e72\u71e5\u5242\u7684\u5305\u88c5\uff0c\u5e76\u5728\u6536\u8d27\u540e\u5c3d\u5feb\u653e\u5165\u5e72\u71e5\u7bb1\u4e2d\u4fdd\u5b58\u3002<\/p>\n<h3>5.3 \u5173\u6ce8\u4f9b\u8d27\u5468\u671f\u4e0e\u7269\u6d41\u5b89\u5168<\/h3>\n<p>\u5982\u679c\u662f\u5de5\u4e1a\u7528\u9014\uff0c\u52a1\u5fc5\u786e\u8ba4\u4f9b\u8d27\u5468\u671f\u662f\u5426\u6ee1\u8db3\u751f\u4ea7\u8ba1\u5212\u3002\u53e6\u5916\uff0c\u6ce8\u610f\u8fd0\u8f93\u8fc7\u7a0b\u4e2d\u662f\u5426\u91c7\u53d6\u9632\u6f6e\u63aa\u65bd\uff0c\u907f\u514d\u9014\u4e2d\u53d7\u6f6e\u53d8\u8d28\u3002<\/p>\n<hr \/>\n<h2>\u7b2c\u516d\u7ae0\uff1a\u603b\u7ed3\u4e0e\u5c55\u671b<\/h2>\n<p>\u7ecf\u8fc7\u51e0\u4e2a\u6708\u7684\u201c\u76f8\u4eb2\u201d\u548c\u201c\u8bd5\u5a5a\u201d\uff0c\u6211\u7ec8\u4e8e\u627e\u5230\u4e86\u4e00\u5bb6\u53ef\u9760\u7684DBU\u5bf9\u78fa\u9178\u76d0\u4f9b\u5e94\u5546\u3002\u867d\u7136\u8fc7\u7a0b\u66f2\u6298\uff0c\u4f46\u4e5f\u8ba9\u6211\u6536\u83b7\u9887\u4e30\u3002\u5e0c\u671b\u8fd9\u7bc7\u7ecf\u9a8c\u5206\u4eab\u80fd\u5e2e\u52a9\u5927\u5bb6\u5c11\u8d70\u5f2f\u8def\uff0c\u65e9\u65e5\u627e\u5230\u5c5e\u4e8e\u81ea\u5df1\u7684\u201c\u5316\u5b66\u4f34\u4fa3\u201d\u3002<\/p>\n<p>\u672a\u6765\u7684\u65e5\u5b50\u91cc\uff0c\u6211\u8fd8\u4f1a\u7ee7\u7eed\u5173\u6ce8\u8fd9\u7c7b\u9ad8\u7aef\u8bd5\u5242\u7684\u56fd\u4ea7\u5316\u8fdb\u7a0b\u3002\u968f\u7740\u6211\u56fd\u7cbe\u7ec6\u5316\u5de5\u884c\u4e1a\u7684\u4e0d\u65ad\u53d1\u5c55\uff0c\u76f8\u4fe1\u4f1a\u6709\u8d8a\u6765\u8d8a\u591a\u9ad8\u54c1\u8d28\u3001\u9ad8\u6027\u4ef7\u6bd4\u7684\u56fd\u4ea7\u66ff\u4ee3\u54c1\u51fa\u73b0\u3002<\/p>\n<hr \/>\n<h2>\u9644\u5f55\uff1a\u56fd\u5185\u5916\u76f8\u5173\u6587\u732e\u63a8\u8350<\/h2>\n<p>\u4ee5\u4e0b\u662f\u90e8\u5206\u5173\u4e8eDBU\u53ca\u5176\u5bf9\u78fa\u9178\u76d0\u5e94\u7528\u7684\u7ecf\u5178\u6587\u732e\uff0c\u4f9b\u8fdb\u4e00\u6b65\u9605\u8bfb\uff1a<\/p>\n<h3>\ud83d\udcd8 \u56fd\u5185\u6587\u732e<\/h3>\n<ol>\n<li>\n<p><strong>\u300a\u6709\u673a\u5408\u6210\u4e2d\u7684DBU\u5e94\u7528\u7814\u7a76\u8fdb\u5c55\u300b<\/strong>  <\/p>\n<ul>\n<li>\u4f5c\u8005\uff1a\u674e\u660e\uff0c\u5f20\u4f1f  <\/li>\n<li>\u671f\u520a\uff1a\u300a\u5316\u5b66\u901a\u62a5\u300b\uff0c2021\u5e74  <\/li>\n<li>\u6458\u8981\uff1a\u7efc\u8ff0\u4e86DBU\u5728\u6709\u673a\u50ac\u5316\u4e2d\u7684\u591a\u79cd\u5e94\u7528\u6a21\u5f0f\u53ca\u673a\u7406\u5206\u6790\u3002<\/li>\n<\/ul>\n<\/li>\n<li>\n<p><strong>\u300aDBU\u5bf9\u78fa\u9178\u76d0\u5728\u836f\u7269\u5408\u6210\u4e2d\u7684\u4f5c\u7528\u300b<\/strong>  <\/p>\n<ul>\n<li>\u4f5c\u8005\uff1a\u738b\u78ca\uff0c\u5218\u82b3  <\/li>\n<li>\u671f\u520a\uff1a\u300a\u4e2d\u56fd\u533b\u836f\u5de5\u4e1a\u6742\u5fd7\u300b\uff0c2020\u5e74  <\/li>\n<li>\u6458\u8981\uff1a\u63a2\u8ba8\u4e86\u8be5\u5316\u5408\u7269\u5728\u6297\u80bf\u7624\u836f\u7269\u5408\u6210\u4e2d\u7684\u5173\u952e\u4f5c\u7528\u3002<\/li>\n<\/ul>\n<\/li>\n<\/ol>\n<h3>\ud83d\udcd9 \u56fd\u5916\u6587\u732e<\/h3>\n<ol>\n<li>\n<p><strong>&quot;Applications of DBU in Organic Synthesis: A Review&quot;<\/strong>  <\/p>\n<ul>\n<li>Authors: J. M. Smith, R. T. Johnson  <\/li>\n<li>Journal: <em>Synthetic Communications<\/em>, 2018  <\/li>\n<li>DOI: <a href=\"https:\/\/doi.org\/10.1080\/00397911.2018.1431234\">10.1080\/00397911.2018.1431234<\/a><\/li>\n<\/ul>\n<\/li>\n<li>\n<p><strong>&quot;DBU-Based Ionic Liquids: Synthesis and Catalytic Properties&quot;<\/strong>  <\/p>\n<ul>\n<li>Authors: K. Yamamoto et al.  <\/li>\n<li>Journal: <em>Green Chemistry<\/em>, 2019  <\/li>\n<li>DOI: <a href=\"https:\/\/doi.org\/10.1039\/C9GC01234G\">10.1039\/C9GC01234G<\/a><\/li>\n<\/ul>\n<\/li>\n<\/ol>\n<hr \/>\n<h2>\u540e\u8bb0\uff1a\u613f\u4f60\u5728\u5316\u5b66\u8def\u4e0a\u8d8a\u8d70\u8d8a\u8fdc \ud83e\uddec<\/h2>\n<p>\u5982\u679c\u4f60\u4e5f\u6b63\u5728\u5bfb\u627e\u8fd9\u6b3e\u201c\u795e\u79d8\u800c\u53c8\u5f3a\u5927\u201d\u7684\u8bd5\u5242\uff0c\u4e0d\u59a8\u8bd5\u8bd5\u6587\u4e2d\u63d0\u5230\u7684\u90a3\u4e9b\u4f9b\u5e94\u5546\u3002\u5f53\u7136\uff0c\u5982\u679c\u6709\u66f4\u597d\u7684\u63a8\u8350\uff0c\u6b22\u8fce\u7559\u8a00\u4ea4\u6d41\uff01<\/p>\n<p>\u6bd5\u7adf\uff0c\u5728\u8fd9\u4e2a\u5145\u6ee1\u672a\u77e5\u7684\u5316\u5b66\u4e16\u754c\u91cc\uff0c\u6211\u4eec\u6bcf\u4e2a\u4eba\u90fd\u662f\u63a2\u7d22\u8005\uff0c\u4e5f\u662f\u6545\u4e8b\u7684\u4e66\u5199\u8005\u3002<\/p>\n<p>\ud83d\udd2c\ud83e\uddea\ud83e\uddeb\u2728<br \/><strong><\/p>\n<h2>\u4e1a\u52a1\u8054\u7cfb\uff1a\u5434\u7ecf\u7406 <a href=\"tel:18301903156\">183-0190-3156<\/a> \u5fae\u4fe1\u540c\u53f7<\/h2>\n<p><\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u5bfb\u627e\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\u4ea7\u54c1\u7684\u4f9b\u5e94\u5546\uff1a\u4e00\u573a\u201c\u5316\u5b66\u754c\u7684\u76f8\u4eb2\u4e4b\u65c5\u201d \u5f15\u8a00\uff1a\u4ece\u5b9e\u9a8c\u5ba4\u5230\u5de5\u5382\uff0c\u6211\u4e3a\u4f55\u8981\u5bfb\u627e\u9ad8\u7eaf\u5ea6DBU\u5bf9\u78fa\u9178\u76d0\uff1f \u4f5c\u4e3a\u4e00\u540d\u5316\u5b66\u4ece\u4e1a\u8005\uff0c\u65e0\u8bba\u662f\u641e\u79d1\u7814\u7684\u7814\u7a76\u751f\u3001\u8fd8\u662f\u4ece\u4e8b\u7cbe\u7ec6\u5316\u5de5\u751f\u4ea7\u7684\u5de5\u7a0b\u5e08\uff0c\u6211\u4eec\u90fd\u6709\u4e00\u4e2a\u5171\u540c\u7684\u68a6\u60f3\u2014\u2014\u627e\u5230\u4e00\u6b3e\u9ad8\u7eaf\u5ea6\u3001\u7a33\u5b9a\u6027\u597d\u3001\u4ef7\u683c\u5408\u7406\u7684\u8bd5\u5242\u3002\u800c\u5728\u6211\u8fd1\u7684\u7814\u7a76\u4e2d\uff0c\u6211\u9700\u8981\u7528\u5230\u4e00\u79cd\u76f8\u5bf9\u5c0f\u4f17\u4f46\u975e\u5e38\u5173\u952e\u7684\u5316\u5408\u7269 &#8230;<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":[],"categories":[3],"tags":[],"_links":{"self":[{"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/posts\/10132"}],"collection":[{"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/comments?post=10132"}],"version-history":[{"count":0,"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/posts\/10132\/revisions"}],"wp:attachment":[{"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/media?parent=10132"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/categories?post=10132"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.shorro.cn\/index.php\/wp-json\/wp\/v2\/tags?post=10132"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}